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Schematic of the 18 kW setup.
Specifications:
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18KW RU 300 Rotoflex Rigaku Rotating Anode
(Purchased new by MRC in 1989)
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Mo Anode (also have choice of Cu, Cr, or Zr)
Zr sputter deposited on Cr target (5/07)-
Line Source (LS): Normal Line Focus
0.5mm x 10 mm, 18 KW max power
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The effective line width is 50
mm due to the 6o take-off angle
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Operating power: 50 KV, 240 mA
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Osmic Max-Flux Optic MF15NP-Mo (MM),
followed by Huber 4-blade slit (S0)
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graded d-spacing parabolic multilayer
collimating mirror. dave= 33.04 Å
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Transmits: Mo Ka1
(0.70932 Å) + Ka2 (0.71361
Å) , Kb/Ka ratio = 5.7x10-4
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Flux=3x108
p/s 0.3mm x 4 mm slit, 10mm beam
height at sample
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0.025¢X divergence,
qave=0.62o,
Dl/l
= 0.04
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( Optional) Si(111) channel-cut (CC)
2-bounce monochromator (also have choice of (220), (004),
(333) )
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Transmits: Mo Ka1 (l
= 0.70932 Å, 10-eV-line-width-2G
->
Dl/l
= 5.7x10-4) Flux=2x107
p/s
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0.001o divergence
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Huber 4-blade incident beam slit (S1)
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2-circle diffractometer (starting from the
bottom to the top)
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Newport translation
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Huber 415 2-circle , w/ 20:1 gear-reducers
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Piezo Torsion-bearing ultra-fine
w-rotation stage for single xtal XSW
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Huber 1003 X-c-f
goniometer
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Sample holder
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2-theta arm w/ guard slit (S2), XIA
filter box, detector slit (S3), Cyberstar NaI X-ray
detector
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Auxillary equipment:
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Goniometer pin
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X-ray Eye
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High-power zoom lens camera
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